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《Chemical Sensors》 2007-02
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Molecular imprinted over-oxidized polypyrrole modified electrode for the detection of 3,4-dihydrobenzoic acid

Wang Gui-lin1,Wang Rong1,2,Wu Xia-qin1,Zhang Zong-rang1 (1.Department of Chemistry,Shanghai Normal University,Shanghai 200234,China) (2.State Key Lab of Chem/Bio Sensing and Chemometrics,Hunan University,Changsha 410082,China)  
Molecular imprinted over-oxidized polypyrrole films modified glassy carbon electrode (3,4-DHBA-OPPy/GC)was prepared by electrochemical polymerization of pyrrole with the cyclic voltammetry in the presence of template molecule,3,4-dihydrobenzoic acid (3,4-DHBA),and was followed by over-oxidized at 1.3 V in phosphate buffer solution (pH=9.05). The modified electrode could successfully avoid the polymerization of oxidized 3,4-DHBA and the interference of 2,4-DHBA. A linear response curve was obtained from 1.0×10-5 mol/L to 1.6×10-3 mol/L,with the detection limit of 5.0×10-6 mol/L.
【Key Words】： 3 4-dihydrobenzoic acid 2 4-dihydrobenzoic acid molecular imprinted polymers (MIP) polypyrrole modified-electrode
【Fund】： 国家自然科学基金(20503016);; 湖南大学生物传感与计量学国家重点实验室开放基金
【CateGory Index】： TP212.2
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