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《Chemistry》 2011-01
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Preparation and Adsorption Performance of Gallium Ion Complex Imprinted Polymers

Zhang Zhaohui1,2,Zhang Huabin1,Hu Yufang1,Li Yanjie1,Nie Lihua2(1College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000;2 State Key Laboratory of Chemo /Biosensing and Chemometrics,Hunan University,Changsha 410082)  
Gallium ions and 8-hydroxyquinoline ternary complex(Gaq3) imprinted polymers were prepared employing acrylamide as functional monomer,ethylene glycol dimethacrylate as crosslinker and 2,2′-azobisisobutyronitrile as initiator in a mixture of chloroform and methanol(V /V,3∶ 2) and characterized by IR and TGA.The adsorption characteristics of as-prepared polymers were evaluated by isotherm adsorption and Langmuir adsorption model.As solid-phase extraction materials,the as-prepared molecularly imprinted polymers can separate and enrich Ga(Ⅲ) from pulverized coal ash successfully with the recovery of 97.36%.
【Key Words】： Molecularly imprinted polymers Gallium Adsorption performance Solid-phase extraction
【Fund】： 湖南省自然科学基金项目(08JJ4004);; 湖南省科技计划项目(2009FJ3009);; 湖南大学化学传感与计量国家重点实验室开放基金项目(2008007);; 林产化工工程湖南省重点实验室开放基金项目(JDZ200903);; 吉首大学研究生科研创新基金项目(JGY200901)资助
【CateGory Index】： O634
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