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《Journal of Jilin University(Science Edition)》 2006-01
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Synthesis and Characterization of β-D-Glucopyranosyl Thiourea

SUN Wei-dong~(1,2),WANG Xiao-ming~2,ZHANG Suo-qin~2,LI Yao-xian~2, ZHENG Ji-fu~2,YUAN Hong~3,GUO Qing-huan~3(1.Department of Chemistry,Chifeng College,Chifeng 024001,Inner Mongolia Autonomous Region,China;2.College of Chemistry,Jilin University,Changchun 130021,China;3.Jilin Chemical Combine Company,Jilin 132021,Jilin Province,China)  
2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl thiourea compounds were synthesised from the reaction of aniline and 2,3,4,6-tetra-O-acetylβ-D-glucopyranosyl isothiocyanate in acetonitrile under reflux.The(2,3,4,6-)tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate was synthesised from 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl bromine.The structures of the title compounds were confirmed by elemental analyses,IR,MS and()~1H NMR spectra.
【Fund】: 国家自然科学基金(批准号:20142002)
【CateGory Index】: O621.2
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