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《Jiangsu Journal of Agricultural Sciences》 2012-01
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Detection of cephalosporins residue in chicken muscles by molecular imprinted solid phase extraction-high performance capillary electrophoresis(MISPE-HPCE)

WANG Xue-yan1,QI Ke-zong2,CHEN Ding-ding3,TAN Hua-rong3,XUE Xiu-heng1(1.Key Laboratory of Analysis and Detection Technology for Food Safety,Hefei 230036,China;2.College of Animal Science,Anhui Agricultural University,Hefei 230036,China;3.Biotechnology Center,Anhui Agricultural University,Hefei 230036,China)  
A fast and accurate method for detecting cephalosporin drugs residues in chicken muscles was established.7-aminocephalosporanic acid molecular imprinted polymers(7-ACA MIP)was synthesized using 7-ACA as template molecules,4-vinylpyridine as functional monomer and ethylene glycol dimethacrylate as cross-linking agent.Cephalosporin drugs(cefalexin,cefradine,cefoperazone and cefazdin) residues in chicken muscles was determined by molecular imprinted solid phase extraction-high performance capillary electrophoresis(MISPE-HPCE),using 7-ACA MIP as solid phase extraction materials.The recoveries of four drugs at different levels were in the range of 78.00%-83.04%,and the relative standard deviations(RSD) were in the range of 2.18%-3.79%.It indicated that MISPE-HPCE method may be suitable for analysis of cephalosporin drugs residues in chicken muscles.
【Key Words】： molecular imprinted solid phase extraction high performance capillary electrophoresis 7-aminocephalosporanic acid cephalosporin drug chicken muscle
【Fund】： 国家十一五科技支撑计划子项目(2006BAK02A08-4)
【CateGory Index】： TQ465.1
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