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《Chinese Journal of Clinical Pharmacy》 2011-05
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Determination of Borneolum syntheticum and(+)-Borneol in Qinbing eyedrop

ZHAO Qiuhua~1,ZHOU Xin~1,GU Xijun~1,HOU Jianwei~2,ZHANG Tong~2(1 Department of Pharmacy,Longhua Hospital, Shanghai University of Traditional Chinese Medicine,Shanghai 200032,China;2 Teaching Experimental Center, Shanghai University of Traditional Chinese Medicine,Shanghai 201203,China)  
AIM To establish a gas chromatography(GC) method for determination of Bomeolum syntheticum and (+)-Borneol in Qinbing eyedrop.METHODS GC analysis was carried out on an Agilent 6890N GC instrument equipped with a flame ionization detector(FID).Separation was performed on a quartz capillary column(19091N-113 HP-INNOWAX Polyethylene Glycol,length 30.0 m,inner diameter 320μm,film thickness 0.25μm) with nitrogen as carrier gas.The column temperature was maintained at 140℃and the temperature of injection port and front detector was 200℃and 230℃,respectively.RESULTS The calibration curves for Bomeolum syntheticum and(+)-Borneol were respectively linear within the range 0.001-0.023 g·L~(-1) with a correlation coefficient(0.999 8) and 0.001-0.08 g·L~(-1)(r=0.999 9).The average recovery of Bomeolum syntheticum was 94.89%.CONCLUSION The method is simple, accurate,rapid and suitable for the determination of volatile ingredients in Qinbing eyedrop.
【Fund】: 上海市卫生局中药新药研发项目(编号2008X002A)
【CateGory Index】: R286.0
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