Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Agrochemicals》 2019-01
Add to Favorite Get Latest Update

Determination of Flufenacet in Water by HPLC

ZONG Fu-lin;XIANG Sheng;YU Zhe;ZHOU Zhi-qiang;College of Science, China Agricultural University;Institute for the Control of Agrochemicals, Ministry of Agriculture and Rural Affairs;  
[Aims] An analysis method using high performance liquid chromatography(HPLC) was developed for the determination of flufenacet in water. [Methods] The water samples were extracted with acetonitrile, followed by quantitative detection by HPLC using Agilent TC-C_(18)(2) column, and with the mixture solution of acetonitrile and 0.1%formic acid water(70∶30, by vol) as mobile phase at 225 nm. [Results] There was a good linear relationship between the target substance concentration and the peak area in the range of 1-100 mg/L. Besides, the average recoveries were89.4-103.1% at the spiked levels of 5 and 50 mg/L, and the relative standard deviations(RSD) were 4.7 and 1.2%,respectively. [Conclusions] The analysis method is simple and convenient, and the accuracy and precision meet with the requirement for pesticide quantitative analysis, which can be applied for determination of flufenacet in water.
【Fund】: 国家自然科学基金项目(31572036)
【CateGory Index】: O657.72;X832
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 1 Hits
1 JIANG Yu-tian, CHEN Tong-ming, LI Mao-qing (Jiangsu Anpon Electrochemical Co., Ltd., Huaian 223002, Jiangsu, China);Synthesis of Flufenacet[J];农药;2007-11
【Co-citations】
Chinese Journal Full-text Database 4 Hits
1 LU Xing-tao;WU Cui-xia;ZHANG Yong;ZHANG Tian-tian;MA Chong;SUN Zhu-bo;KONG Fan-hua;Taian Academy of Agricultural Sciences of Shandong Province/Development and Promotion Centre for New Herbicide Technology of Shandong Province;;Efficacy of Bacara Forte 360 SC on Weeds in Winter Wheat Fields and Its Safety to Succeeding Crops[J];杂草科学;2013-04
2 ZHOU Xin-jian;HAN Bang-you;LI Mei-fang;Department of Technology,Jiangsu Kuaida Agrochemical CO.,Ltd.;;Improvement on the Synthesis Process of Flufenacet[J];南通职业大学学报;2013-04
3 JI Ming(School of Chemistry and Chemical Engeering,Huaiyin Normal University,Huaian Jiangsu 223300,China);New Process for the Preparation of N-isopropyl-p-fluoroaniline[J];淮阴师范学院学报(自然科学版);2009-03
4 CHENG Si-xi, DU Sheng-hua (Hunan Research Institute of Chemical Industry, Changsha 410007, China);Synthesis of 2-Methylsulfonyl-5-tirfluoromethyl-1,3,4-thiadiazole[J];农药;2009-04
【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 Li Yusheng et al. (Jiangsu Pesticide Research Institute, Nanjing 210036);Synthesis of a New Herbicide Flufenact[J];现代农药;2002-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved