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《Jiangxi Chemical Industry》 2005-02
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Research on Synthesis and Purification of Jasminaldehyde

GUAN Shi-lon1 ZItOU Guo-Fei2 (1. Hubei Key Lab of Novel Chemical Reactor and Green Chemical Technology, Wuhan 430074, China; 2. Institute of Jiangxi Light Industry, Nanchang 330029, China)  
Jasminaldehyde was synthesised by the aldol condensation of benzaldehyde with heptanal under the condition of BTEAC as phase transfer catalyst, DMF as cocatalyst and anhydrous K2CO3 as base catalyst with the yield beyond 85% The qualitative analysis by TLC and purification by CLC of Jasminaldehyde were studied. The constructon of jasminaldehyde was characterized by IR and 1?HNMR .
【CateGory Index】: TQ655
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【References】
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1 LI Chong1,CHEN Xu-dong2,LIAO Zheng-fu3(1 College of Chemical Engineering and Material Science,Zhuhai Campus of Beijing Institute of Technology,Zhuhai 519085;2 Institute of Polymer Science,School of Chemistry and Chemical Engineering,Sun Yat-Sen University,Guangzhou 510275;3 Faulty of Materials and Energy,Guangdong University of Technology,Guangzhou 510090,China);Recent Research Development of Jasminaldehydes Synthesis Methods[J];Guangzhou Chemical Industry;2008-02
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1 GUAN Shilong~1,FANG Jide~1,YANG Yi~2(1.School of Chemical Engineering and Pharmacy,Wuhan Institute of Chemical Technology,Wuhan 430074,China; 2.Instrument Analysis Center of Guangxi Normal University,Guilin 541004,China);Quantitative determination of jasminal by gas chromotography[J];Journal of Wuhan Institute of Chemical Technology;2005-01
2 HUANG Wen-Bang~* GUAN Shi-Long (Department of Chemistry,Guangxi Normal University,541004 Guilin,Guangxi);A Modified Phase Transfer Catalyzed Synthesis of Jasmaldehyde[J];Chinese Journal of Organic cHEMISTRY;1991-05
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1 Zhang Youjin Lu Chuanhua(Hefei lnstitute of Economics and Technlogy) (Anhui Traditional Chinese medicine Collede)Xu Zhiqang;Li Han;Xie fuxing(Depe. of Chemistry);Synthesis of αand βLonone[J];JOURNAL OF ANHUI UNIVERSITY(NATURAL SCIENCES);1994-03
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1 GUAN Shi-long~1,HUANG Wen-bang~2(1.Hubei Key Lab of Novel Chemical Reactor and Green Chemical Technology,Wuhan 430074,China;2.Department of Chemistry and Chemical Engineering,Guangxi Normal University,Guilin 541004,China);Solid-liquid phase transfer catalytic synthesis of α-alkyl cinnamaldehyde products[J];China Surfactant Detergent & Cosmetics;2006-01
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【Secondary Citations】
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1 HUANG Wen-Bang~* GUAN Shi-Long (Department of Chemistry,Guangxi Normal University,541004 Guilin,Guangxi);A Modified Phase Transfer Catalyzed Synthesis of Jasmaldehyde[J];Chinese Journal of Organic cHEMISTRY;1991-05
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