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《Jiangxi Chemical Industry》 2005-02
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The study of Method For Determination Of water-soluable As(Ⅲ) And As(V) in soil By Hydride Generation Atomic Fluorescence Spectrometry (HG-AFS)

Chen Jin-Feng Gao Guo-Wei (1. Faculty of earth resources and environment engineering, Wuhan university of science and technology, Wuhan 430062 2.Faculty of material and chemical engineering, Jiangxi university of science and technology, jiangxi ganzhou 341000)  
The method for determination of As(III) and As(V) by hydride generation atomic fluorescence spectrometry (HG-AFS) was described. The content of As(III) and total arsenic in samples were determined by HG AFS in the medium of 1% (V/V) hydrochloric acid solution, and the concentration of As(V ) can be calculated by the difference of them, and the separation of As(III)and As(V) by anion ion-exchange resin was studied as well. The effect of carrier gas flow-rate,sodium tetrahydroborate concentration and conditions of ion-exchange was investigated. The method was simple, rapid, reliable and accurate. The detection limit (DL) was 0.10ng. The method was applied to determine the arsenic species in soil samples and the result was satisfactory.
【CateGory Index】: S151.9
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