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《Journal of Synthetic Crystals》 2006-06
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Synthesis,Crystal Structure and Spectral Characterization of the Complex[Zn(CH_3CH_2CH_2CH_2N=CHC_6H_4O)_2]

MA Wei-xing~(1,2),QIAN Bao-hua~2,CHEN Jun~2,SHA Ou~2,XU Xing-you~2 (1.Jiangsu Provincial Key Laboratory of Ocean Biotechnology,Huaihai Institute of Technology,Lianyungang 222005,China;2.Department of Chemical Engineering,Huaihai Institute of Technology,Lianyungang 222005,China)  
A new complex [Zn(CH_3CH_2 CH_2CH_2N=CHC_6H_4O)_2]~1 was synthesized based on the reaction of zinc(II) acetate,salicylal and n-butylamine in methanol medium.The structure of the complex was confirmed by IR,~1H NMR,elemental analysis and thermal analysis.The crystal structure of the complex was also determined by X-ray single crystal diffraction.The crystal belongs to tetragonal system with space group P-4,and crystallographic data of the compound are: a=1.4380(2)nm,b=(1.4380(2)nm),c=0.53803(18)nm,α=β=γ=90°,V=1.1126(4)nm~3;D_c=1.247g/cm~3;Z=2;F(000)=400;μ=1.12mm~(-1).Zinc(Ⅱ) atom lies at the center of a distorted tetrahedral coordination consisting of two N atoms and two O atoms from two schiff bases.
【Fund】: 江苏省高校自然科学研究计划(No.05KJB150003);; 淮海工学院江苏省海洋生物技术重点建设实验室基金(No.2005HS010);; 淮海工学院学科基金资助项目(No.XK200310)
【CateGory Index】: O641.4
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