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《Journal of Synthetic Crystals》 2014-01
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Solid-phase,Liquid-phase Synthesis and Crystal Growth of a Nonlinear Optical Material Ca_9Y_(0. 5)La_(0. 5)(VO_4)_7

SUN Shi-jia;LIN Zhou-bin;ZHANG Li-zhen;HUANG Yi-sheng;WANG Guo-fu;Key Laboratory of Optoelectronic Materials Chemistry and Physics,Fujian Institute of Research on the Structure of Matter,Chinese Academy of Sciences;  
The polycrystalline materials of Ca9Y0. 5La0. 5( VO4)7were prepared by methods of solid-phase and liquid-phase synthesis,respectively. The Ca9Y0. 5La0. 5( VO4)7crystals with dimensions of 30 mm × 33 mm( solid-phase synthesis) and 20 mm × 27 mm( liquid-phase synthesis) were grown by the Czochralski method successfully. The transmittance of the grown crystals in the UV-VIS-NIR range was measured,and the second harmonic generation efficiency of Ca9Y0. 5La0. 5( VO4)7crystal was measured by the Kurtz powder method. The results indicate that the latter has 10% higher transmittance than that of the former. The second harmonic efficiency is about 1. 8 times and 2. 5 times as large as that of KDP crystal for the former and the latter,respectively. The chemical etching of the crystals shows that there is less defect in the crystal grown from liquid-phase synthesis materials. These results reveal that the liquidphase synthesis can improve the optical quality of the crystal.
【Fund】: 国家自然科学基金(61275177 61108054 51302260)
【CateGory Index】: O782
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