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《Journal of Synthetic Crystals》 2014-01
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Mannitol-assisted Hydrothermal Synthesis and Photocatalytic Performance of BiPO_4

XING Xin-yan;DING Hui-fang;FAN Guang-yan;XI Guo-xi;ZHU Gui-fen;School of Chemistry and Chemical Engineering,Henan Normal University;School of Environment,Henan Normal University;  
BiPO4photocatalysts were prepared by mannitol-assisted hydrothermal method and the photocatalytic acitivities for degradating rhodamine B were investigated. The BiPO4products were characterized by XRD,SEM,FTIR and UV-vis DRS and N2adsorption techniques. The results show that the addition of mannitol doesn't change the crystal structure of the product. But Prismatic BiPO4changes into polyhedral BiPO4when hydrothermal reaction takes place at 170 ℃ for 24 h. Moreover,the size of polyhedron decreased with an increase in the addition amount of mannitol. A further increase might result in the hierarchical structure. Lower hydrothermal temperature or shorter time makes for hexagonal phase BiPO4in rod-like shape with protuberances on its cross sections. Higher temperature or longer time makes for monoclinic phase. Nevertheless,the crystallinity degrees are both high. Monoclinic product formation experiences a hexagonal phase transition. There is no mannitol molecule but crystal water in products. The monoclinic BiPO4obtained at 170 ℃ with mannitol assistance shows the highest photocatalytic activity,which is superior to that of the BiPO4obtained without mannitol assistance. The hexagonal one obtained at 110 ℃ shows the lowest activity. Light response range may be the reason for the different photocatalytic activity.
【Fund】: 国家自然科学基金(51174083);; 教育部高等学校博士学科点专项科研基金(20114104110004);; 河南省基础与前沿技术研究(122300410283);; 河南省重点科技攻关项目(132102210436);; 河南省教育厅自然科学研究计划项目(2011B150018)
【CateGory Index】: O643.36
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【Citations】
Chinese Journal Full-text Database 6 Hits
1 YANG Kai1,YU Chang-lin1,ZHANG Li-na1,YU Ji-mei2(1.School of Metallurgy and Chemical Engineering,Jiangxi University of Science and Technology,Ganzhou 341000,China;2.Department of Chemistry,Chinese University of Hong Kong,Hong Kong,China)(Received 8 August 2011,accepted 19 August 2011);Hydrothermal Synthesis and Photocatalytic Performance of BiOCl/ZnO Heterojunction Photocatalysts[J];Journal of Synthetic Crystals;2012-01
2 TANG Jie,ZHAN Hong-quan,JIANG Xiang-ping,XU Ming-zhu,LI Xiao-hong(Jiangxi Key Laboratory of Advanced Ceramic Materials,Jingdezhen Ceramic Institute,Jingdezhen 333001,China)(Received 6 December 2012,accepted 17 January 2013);Preparation and Photocatalytic Activity of Bi_2WO_6 by Hydrothermal Method with Differrent Acid-assited[J];Journal of Synthetic Crystals;2013-06
3 WEI Yong-ge,CHEN Ying,ZHANG Qiang,WANG Kun,XU Lei(School of Materials Science and Technology,Changchun University of Science and Technology,Changchun 130022,China)(Received 7 March 2013,accepted 4 April 2013);Preparation and Photocatalytic Properties of RGO-BiVO_4 Composite[J];Journal of Synthetic Crystals;2013-06
4 DING Liu-liu;JIANG Guo-jian;LI Wen-jun;LIU Yun-ying;FENG Yun-fei;School of Materials Science and Engineering,Shanghai Institute of Technology;Department of Chemistry,Tongji University;Med-X Research Institute in School of Biomedical Engineering,Shanghai Jiaotong University;;Study on Photocatalytic Properties of BiFeO_3 Prepared by Hydrothermal Method[J];Journal of Synthetic Crystals;2013-08
5 LIU Yan-Fang 2 MA Xin-Guo 1 YI Xin 3 ZHU Yong-Fa 1, ( 1 Department of Chemistry,Tsinghua University,Beijing 100084,P.R.China; 2 College of Science,Beijing University of Chemical Technology,Beijing 100029,P.R.China; 3 Department of Chemistry,Shanghai Normal University,Shanghai 200234,P.R.China);Controllable Synthesis and Photocatalytic Performance of Bismuth Phosphate Nanorods[J];Acta Physico-Chimica Sinica;2012-03
6 ZHU Yan-Yan 1,2 LIU Yan-Fang 1 LU Yan-Hui 1 WANG Hua 2 LING Qiang 2 ZHU Yong-Fa 1,(1 Department of Chemistry,Tsinghua University,Beijing 100084,P.R.China;2 Institute of Aeronautical Meteorology and Chemical Defence,Equipment Academy of Air Force,Beijing 100085,P.R.China);Reflux Preparation and Photocatalytic Performance of Bismuth Phosphate Nanorods[J];Acta Physico-Chimica Sinica;2013-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHENG Yunlong;ZHAO Minglei;LI Liping;LI Guangshe;ZHANG Xitian;School of Physics and Electronic Engineering,Harbin Normal University;Fujian Institute of Research on the Structure of Matter,Chinese Academy of Sciences;;Preparation,Phase Structure Control and Luminescent Properties of Bi_(1-x)Eu_xPO_4 Nanophosphors[J];Chemical Journal of Chinese Universities;2014-05
2 XIONG Shiwei;FANG Yanfen;LI Xinyu;LI Ruiping;HUANG Yingping;Engineering Research Center of Eco-environment in Three Gorges Reservoir Region,Ministry of Education,China Three Gorges University;Collaborative Innovation Center for Geo-Hazards and Eco-Environment in Three Gorges Area;;Synthesis of BiPO_4 and its photocatalytic degradation rhodamine B toxic organic pollutants[J];Environmental Chemistry;2013-10
3 ZHAO Rong-xiang1,LI Xiu-ping2,XU Zhu-de3(1.College of Petrochemical Engineering,Liaoning University of Petroleum & Chemical Technology,Fushun 113001,China; 2.College of Chemistry & Material Science Engineering,Liaoning University of Petroleum & Chemical Technology,Fushun 113001,China; 3.Institute of Physical Chemistry,Department of Chemistry,Zhejiang University,Hangzhou 310027,China);Effect of Ionic Liquids on Photocatalytic Performance and Particle Size of CdS[J];Journal of Synthetic Crystals;2012-04
4 XU Xiu-quan1,3,WU Chun-du2,3(1.College of Pharmacy,Jiangsu University,Zhenjiang 212013,China;2.Yangzhou Vocational College of Environment and Resources,Yangzhou 225002,China;3.College of Environment,Jiangsu University,Zhenjiang 212013,China);Preparation of Ag@AgBrH_2WO_4 Heterojunction Photocatalyst and Its Performance for Degradation of Moxifloxacin Hydrochloride under Visible-Light Irradiation[J];Journal of Synthetic Crystals;2012-06
5 ZHANG Xu-dong,ZHANG Xue-guang,HE Wen,LI Hai-ming,BI Zhi-ying,WANG Zhuo(Shandong Polytechnic University,Ji′nan 250353,China);Preparation and Characterization of Mesoporous Spherical LiFePO_4/C in Situ Composite Materials[J];Journal of Synthetic Crystals;2013-04
6 YU Chang-lin;LI Xin;ZHOU Wan-qin;FAN Qi-zhe;WEI Long-fu;CHEN Jian-chai;School of Metallurgy and Chemical Engineering;School of Information Engineering,Jiangxi University of Science and Technology;;Preparation,Characterization and Photocatalytic Performance of Al~(3+) Doped ZnS Nanocrystals[J];Journal of Synthetic Crystals;2013-12
7 BAI Li-jing;KOU Gang;GONG Zhen-yao;ZHAO Zhi-ming;College of Materials Science and Engineering,Xi'an University of Technology;;Study on Photocatalytic Activity of TiO_2-ZnO Heterojunction Composite Films with Different Structure[J];Journal of Synthetic Crystals;2013-12
8 CHEN Yuan;YANG Jia-tian;XIE Zu-fang;WEI Qing-min;ZHU Li-gang;LIU Guo-cong;College of Chemistry and Material,Yulin Normal University;Guangxi Experiment Centre of Science and Technology( Guangxi University);Department of Chemical Engineering,Huizhou University;;Preparation and Photocatalytic Performance of Egg-tart-like Bi_2WO_6 Catalysts[J];Journal of Synthetic Crystals;2014-02
9 MA Long-tao;YU Xiao-hong;LU Can;MENG Da-wei;WANG Yong-qian;XUE Qiang;YOU Lei;Faculty of Material Science and Chemistry,China University of Geosciences;;Preparation and Photocatalytic Properties of Fe-doped Nanometer ZnO[J];Journal of Synthetic Crystals;2014-01
10 WANG Dan-jun;YUE Lin-lin;ZHANG Jie;HE Xiao-mei;GUO Li;FU Feng;Key Laboratory of Chemical Reaction Engineering of Shaanxi,Department of Chemistry and Chemical Engineering,Yan'an University;;Synthesis of Rod-like BiPO_4 Microcrystalline and Its Photocatalytic Oxidative Desulfurization(Photo-ODS)Activity of Simulation Fuel[J];Journal of Synthetic Crystals;2014-01
China Proceedings of conference Full-text Database 1 Hits
1 Yanyan ZHU,Yongfa ZHU,Yanfang LIU,Qiang LING;Study of high-active BiPO_4 photocatalysts by heating under refluxing synthesis[A];[C];2012
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 XIAO Yi1, DANG Liqin1, AN Lizhen1, BAI Shiying1, LEI Zhibin1,2(1 Institute of Chemistry for Functionalized Materials, Faculty of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, Liaoning, China; 2 State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, Fujian, China);Photocatalytic Degradation of Rhodamine B and Phenol by TiO_2 Loaded on Mesoporous Graphitic Carbon[J];Chinese Journal of Catalysis;2008-01
2 LI Changquan1,2, LUO Laitao2,, XIONG Guangwei2 1School of Material Science and Engineering, Nanchang University, Nanchang 330031, Jiangxi, China 2Institute of Applied Chemistry, Nanchang University, Nanchang 330031, Jiangxi, China;Optical Properties of ZnO Nanotubes and Their Photocatalytic Activity for Degradation of Methyl Orange[J];Chinese Journal of Catalysis;2009-10
3 YU Changlin1,,YANG Kai1,SHU Qing1,YU Jimmy C2,CAO Fangfang1,LI Xin1 1School of Materials and Chemical Engineering,Jiangxi University of Science and Technology,Ganzhou 341000,Jiangxi,China 2Department of Chemistry,The Chinese University of Hong Kong,Hong Kong,China;Preparation of WO_3/ZnO Composite Photocatalyst and Its Photocatalytic Performance[J];Chinese Journal of Catalysis;2011-04
4 XIAN Tao1,2,YANG Hua1,2,,DAI Jianfeng1,2,WEI Zhiqiang1,2,MA Jinyuan2,FENG Wangjun2 1State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials,Lanzhou University of Technology,Lanzhou 730050,Gansu,China 2School of Science,Lanzhou University of Technology,Lanzhou 730050,Gansu,China;Preparation and Photocatalytic Performance of Nano-bismuth Ferrite with Tunable Size[J];Chinese Journal of Catalysis;2011-04
5 CHEN Yuan1,2,LIU Guocong1,3,LI Zhiyou2,HUANG Suping,ZHOU Kechao2,* 1Institute of Advanced Materials & Chembiosensing Technology,Yulin Normal University,Yulin 537000,Guangxi,China 2State Key Laboratory of Powder Metallurgy,Central South University,Changsha 410083,Hunan,China 3College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,Hunan,China;Citric Acid-Assisted Hydrothermal Synthesis of Bi_2WO_6 Nanosheets for Highly Efficient Degradation of Methyl Orange under Visible Light Irradiation[J];Chinese Journal of Catalysis;2011-10
6 JI Tian-hao,YANG Fang,ZHOU Jiao-yan,DU Hai-yan,SUN Jia-yue College of Chemical and Environmental Engineering,Beijing Technology and Business University,Beijing 100048,China;Visible-Light Responding BiVO_4/TiO_2 Nanocomposite Photocatalyst[J];Spectroscopy and Spectral Analysis;2010-07
7 GE Lei,CUI Lishan (Department of Materials Science and Engineering, China University of Petroleum (Beijing), Beijing 102249, China);PREPARATION AND PHOTOCATALYTIC PERFORMANCE OF NOVEL PALLADIUM OXIDE/ BISMUTH VANADATE VISIBLE LIGHT INDUCED COMPOSITE PHOTOCATALYSTS[J];Journal of the Chinese Ceramic Society;2008-03
8 ZHOU Yin1,2,WANG Yu1,LU Shi-xiang1,XU Wen-guo1,SU Su1(1.Institute of Science,Beijing Institute of Technology,Beijing 100081,China;2.Headquarters,Chengdu Municipal Fire Brigade,Chengdu 610000,China);Photocatalytic Degradation of Reactive Brilliant Blue X-BR with La~(3+),Al~(3+) Co-doped ZnO Nano-particles[J];Journal of Synthetic Crystals;2009-04
9 LI Bo,SUN Hua-jun,CHEN Wen,ZHANG Cheng-yong,SHEN Jie,ZHOU Jing(School of Materials Science and Engineering,Wuhan University of Technology,Wuhan 430070,China);Study on Phase Transition of BiFeO_3 Powders Prepared by Hydrothermal Method[J];Journal of Synthetic Crystals;2010-01
10 XING Guang-jian1,LI Yu-mei1,ZHAO Zheng1,WANG Yi2,WU Guang-ming1(1.Department of Materials Science and Engineering,Beijing Institute of Petrochemical Technology,Beijing 102617,China;2.Department of Mathematics and Physics,Beijing Institute of Petrochemical Technology,Beijing 102617,China);Preparation and Photocatalytic Properties of Bismuth Tungsten Oxide Nanomaterials with Different Morphologies[J];Journal of Synthetic Crystals;2010-05
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