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《Journal of Synthetic Crystals》 2014-01
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Study on the Carbonation of Pre-sintered Hydroxyapatite

ZHU Qing-xia;WU Jian-qing;Jingdezhen Ceramic Institute;College of Materials Science and Engineering,South China University of Technology;  
Based on the research of the effect of pre-sintering temperature of hydroxyapatite on the hydroxyl and phase,the effects of the following carbonation treatment atmosphere and time on carbonate substitution were investigated. The phase composition of the powders were characterized by X-ray diffraction,and the content and type of the carbonate substitution were analyzed using carbon-sulfur elemental analysis and fourier transform infrared spectroscopy,respectively. The results show that hydroxyapatite gradually releases its OH-with increasing the pre-sintering temperature. The carbonate ions can substitute the hydroxyl to form carbonated hydroxyapatite with prevalence to A-type substitution. Carbonation effect of hydroxyapatite improves with the residual hydroxyl content increses. Wet atmosphere can stabilize the hydroxyl and carbonate content increases with extending the treatment time in asymptote form.
【Fund】: 江西省自然科学基金(20122BAB206008);; 江西省青年科学家资助项目(20122BCB23019)
【CateGory Index】: R318.08
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