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《Journal of Synthetic Crystals》 2015-01
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Preparation of ZTA Porous Ceramics by TBA Based Gel-casting

GE Xing-ze;WANG Shu-bin;XIAO Xiong-fu;Key Laboratory of Aerospace Materials and Performance,Ministry of Education,School of Materials Science and Engineering,Beihang University;  
ZTA porous ceramics were fabricated by tert-butyl alcohol-based gel-casting process,using acrylamide as monomer. The technological parameters of molding process,such as the solid content,the concentration of pre-mixed solution,the dosage of initiator and the curing temperature were optimized.The effect of the sintering temperature and the holding time on the porous ceramic porosity and the distribution of pore size were analyzed. The results show that a porous ceramic with porosity as 59. 05%and most probable pore size of 0. 72 μm is sintered at 1500 ℃ for 2 h with the solid content as 10vol%,the content of pre-mixed solution as 15wt%,the dosage of initiator as 20wt%,curing temperature as 40℃ respectively. Meanwhile,the 87. 22% pore size is within 0. 40-5. 00 μm and the compressive strength of ZTA porous ceramic is 56. 09 MPa.
【CateGory Index】: TQ174.62
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