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《Journal of Synthetic Crystals》 2015-01
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Study on Preparation and Spinnability of Spinning Solution for Polycrystalline Mullite Fiber

JING Gui-hua;ZHANG Yu-jun;LI Cheng-shun;QIAO Wen-guang;Key Laboratory for Liquid Structure and Heredity of Materials,Ministry of Education,Shandong University;Shandong Luyang Share Co. ,Ltd;  
The spinning solution for polycrystalline mullite fiber was prepared by sol-gel method,using aluminum powders,HCl and silica sol as raw materials,deionized water as solution. The effect of the amount of PVA on the spinnabiltiy of sol was inspected. The infrared absorption characteristics and the behavior of rheology of the spinning sole were studied respectively by infrared absorption spectra of FTIR and rotational rheometer. The phase composition of the precursor fibers after heat treatment was analyzed with the help of XRD. The results show that the sol is non-newtonian fluid with shear thinning property and presents no tube siphon phenomenon when the amount of additives of PVA is in the range of 2%-4%. The sol with solid content in the 30%-40% and viscosity in the 4-7 Pa · s has excellent spinnability,with sol spinnability index of 25-26 cm /s. In the spinning sol there are linear polymer chain structures of Al-O-Si,which are benefit to spinning. The main crystal phase of fiber calcined at 1050 ℃is mullite.
【Fund】: 山东省自然科学基金(51072099)
【CateGory Index】: TQ343
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【Citations】
Chinese Journal Full-text Database 10 Hits
1 WANG Li-wang,WANG Jia-bang,YANG Hui,MAO Yu-xiong,CHEN Gui-hua(Department of Materials Science and Engineering,Zhejiang University,Hangzhou 310027,China);Preparation and Crystallization of Si-Al Gel[J];Journal of Materials Science and Engineering;2006-03
2 Chen Guihua Liang Huading (Taizhou University Zhejiang Linhai 317000);Preparation of Mullite Powder by Sol-Gel Process[J];;2005-11
3 Hong-bin Tan School of Materials Science and Engineering,Shaanxi University of Technology,Hanzhong 723003,China;Preparation of long alumina fibers by sol-gel method using tartaric acid[J];矿物冶金与材料学报(英文版);2011-06
4 Fu Shunde,Xu Jianfeng,Liu Libin,et al Henan Key Laboratory of Advanced Refractories,Sinosteel Luoyang Institute of Refractories Research Co.,Ltd.,Luoyang 471039,Henan,China;Influence of colloidal viscosity and fiberization process conditions on properties of 80 polycrystalline alumina fiber[J];Refractories;2010-02
5 ZHANG Ya-bin,Ding Ya-ping,GAO Ji-qiang,YANG Jian-feng(State Key Laboratory for Mechanical Behavior of Materials,Xi'an Jiaotong University,Xi′an 710049,China);Research on Preparation Technology of Mullite Continue Fibers Prepared by Sol-gel Method[J];Journal of Synthetic Crystals;2009-S1
6 YANG Tao-feng, LI Yao-jun, CHEN Da-jun (State Key Lab of Fiber Materials Modification, Donghua University,Shanghai 200051,China);Rheological behavior of the chip for melt-spinning polyurethane fibers[J];China Elastomerics;2002-05
7 LI Cheng-Shun,ZHANG Yu-Jun,ZHANG Jing-De(School of Materials Science and Engineering,Shandong University,Jinan 250061,China);Polycrystalline Mullite Fibers Prepared by Sol-Gel Method[J];Journal of Inorganic Materials;2009-04
8 HUANG Qian-jun,CHEN Xiao-jun,CHEN Li-fu(Department of Materials Science and Engineering,Xiamen University,Xiamen 361005,China);Preparation of the Polycrystalline Alumina Fubers by Sol-gel Progress[J];Journal of Xiamen University(Natural Science);2006-03
9 LI Cheng-Shun1 ZHANG Yu-Jun,1 LU Cheng-Hong2 LIU Chao2(1Key Laboratory of Engineering Ceramics,School of Materials Science and Engineering,Shandong University,Jinan 250061)(2Crystalline Fiber Institute of Luyang,Shandong Luyang Co.,Ltd,Zibo,Shandong 256120);Preparation,Structure and Rheological Behavior of Yttrium Aluminum Garnet Fiber Precursor[J];Chinese Journal of Inorganic Chemistry;2009-04
10 Wang Shufeng,Liu Liqiang,Ji Minxia,Li Zhenyi(College of Material Science and Engineering of Shangdong University of Science and Technology,Shandong Qingdao 266510,China);The characteristics of spinnable mullite sol prepared by sol-gel method[J];Inorganic Chemicals Industry;2005-12
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Chen Xiaoyuan1, Wang Gang1,2, Lu Ai1, Yu Xuejiang1(1.Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang 621900, China;2.Sichuan Coremer Materials Co. Ltd., Mianyang 621000, China);COMPATIBILITY AND MECHANICAL PROPERTIES OF PEEK/PPS[J];Engineering Plastics Application;2007-02
2 Jin Gang,Yin Xiaochun,He Guangjian,Liang Yong(National Engineering Research Center of Novel Equipment for Polymer Processing,South China University of Technology,Guangzhou 510641,China);DEVELOPMENT OF LONG GLASS FIBRE REINFORCED THERMOPLASTIC INJECTION MOLDING TECHNOLOGY[J];Engineering Plastics Application;2007-09
3 Chen Aodong(University of Shanghai for Science and Technology,Shanghai 200093,China);CAE ANALYSIS OF PLASTIC CLASP FILLING PROCESS[J];Engineering Plastics Application;2009-11
4 Min Min1,Lu Ai2,Dai Houyi1,Gao Yong1,Yu Dahai1(1.Sichuan Huatong Research Center for Special Engineering Plastics,Chengdu 610041,China;2.Institute of Chemical Materials,China Academy of Engineering Physics,Mianyang 621900,China);COMPATIBILITY AND NON-ISOTHERMAL CRYSTALLIZATION KINETICS OF PPS/GB[J];Engineering Plastics Application;2010-01
5 Zhang Zhijian,Zhang Jianzhong (Jushi Fiberglass Research Institute,Zhejiang Key Laboratory for Fiberglass Research,Jushi Group Co.Ltd.,Tongxiang 314500,China);DEVELOPMENT AND APPLICATION OF PA66/GF COMPOSITES[J];Engineering Plastics Application;2010-08
6 XU Li HU Zhi an (Baosteel Multiple Development Co.,Shanghai China,201900);Discussion on Development Prospect of Slag Wool Production[J];Bao Steel Technology;2002-04
7 ZHOU Chao1,ZHENG Ya1,ZHANG Jia-xian1,FAN Hong-jie2(1.School of Mechanical Engineering,Nanjing University of Science and Technology,Nanjing 210094,Jiangsu,China;2.Xi'an Modern Chemistry Research Institute,Xi'an 710065,Shaanxi,China);Analysis of Stress Relaxation Spectrum of Pasty Propellant[J];Acta Armamentarii;2008-05
8 LIU Zhao-miao,LIU Xin,WANG Guo-bin(College of Mechanical Engineering and Applied Electronics Technology,Beijing University of Technology,Beijing 100124,China);Analysis on Vortex in Drag Creeping Laminar-flow of Coating Fluids Between Plates[J];Journal of Beijing University of Technology;2011-08
9 LIANG Zhong-quan 1,XUE Yuan-de 1,DONG He-ying 2 (1.School of Aerospace Engineering,Tongji University,Shanghai 200092,China; 2.Nanjing Fiberglass Research Design Institute,Nanjing 210012,China);EFFECTS OF FILAMENT DIAMETER AND SIZING AGENT ON PROPERTIES OF HIGH STRENGTH GLASSFIBER AND COMPOSITES[J];Fiber Reinforced Plastics/Composite;2004-05
10 LI Wei-jun,CAI Feng,TANG Yu;Introduction of Design and Operation about 88m~2 Producer Gas Fired End Port Medium-Alkali Fiber Glass Melting Furnace[J];Glass & Enamel;2011-04
China Proceedings of conference Full-text Database 10 Hits
1 Dong Ruijiao~1,Keuser Marcus~2,Zhang Youwei,Zhao Jiongxin~1,Wu Chengxun~1,Pan Ding~1 (1 State key laboratory for modification of chemical fiber and polymer materials, Donghua University,Shanghai 200051; 2 School of Applied Chemistry,Reutlingen University,Reutlingen D-72762,Germany);Coagulation Formation and Phase Separation of The Precursor of Polyacrylonitrile-Based Carbon Fiber[A];[C];2008
2 Erke Wang,HuiFang Chen,Ding Pan (State Key Laboratory for Chemical Fibers Modification and Polymer Materials, Donghua University,Shanghai 201620);Investigating the Spinnability in the Dry-jet Wet Spinning and the Wet Spinning of PAN/DMSO System[A];[C];2008
3 GUO Zhen-hua~(1,2) LIU Bo~1 (1.College of Postdoctoral Mechanical Engineering ,Hebei University of Technology,Tianjin 300130,China; 2.College of Energy and Environmental Engineering,Hebei University of Technology,Tianjin 300401,China);Study on preparation and properties of dolomite/fly ash fibers[A];[C];2007
4 Li YI,SHU Yu-guang,LIANG Ji-cai,SUN Guo-en,LI Ming (Key Laboratory of Automobile Materials,Ministry of Education,Jilin University,Changchun 130025,China);The study of cell growth in microcellular injection molding processing[A];[C];2010
5 Zhao ke (The engineering research center of fibre composite building material and structure of the Ministry of Education. Zhengzhou University,Zhengzhou 450002);The bending equation for steel bar and FRP rebar[A];[C];2009
6 Wu Qiye Feng Shaohua Mu Jinxia Zhang Na Wang Dujin (Key Laboratory of Rubber-Plastics, Ministry of Education, Qingdao University of Science and Technology, Qingdao, 266042, China);The Rheology of several PP Samples prepared by Reactive Extruded Degrading[A];[C];2006
7 Mu Jingxia Wang Ning Zhao bei Li Peng Wu Qiye Yin Jinghua (Key laboratory of Rubber-Plastics, Ministry of Education, Qingdao University of Science and Technology, Qingdao, 266042, China);The Rheology of Graft LLDPE Prepared by Reactive Extrusion[A];[C];2006
8 CHEN Xiaoyuan, LU Ai, Yu Xuejiang (Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang 621900);Rheological behavior and compatibility of PEEK/PPS Blends[A];[C];2006
9 JIANG Aimin~*,YU Shengchun,ZOU Changqing,TIAN Aiping (Department of Airborne Vehicle Engineering,Naval Aeronautical and Astronautical University,Yantai,264001,China);Numerical Simulation of Composite Solid Propellant Slurry Mixing in Kneading Mixer[A];[C];2010
10 LIAO Huayong~*,TAO yu,TAO Guoliang (Polymer Materials Key Laboratory of Changzhou City,Changzhou University,Changzhou,213164,China);Wall slip behavior of HDPE/LDPE polymer blends[A];[C];2010
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Xue Mingjun; Zhou Shigui; Wang Cong; Qiu Tian; Zhao Yanhua; Feng Junjun(East China University of Science and Technology);Investigation of the Spinnability of Inorganic Alumina Solution[J];GLASS & ENAMEL;1994-05
2 ZHANG Nan CHEN Lei HU Zuming ZHU Jing LIU Zhaofeng (Man-Made Fiber Research lnstitute,Donghua University,Shanghai 200051);Study on Flow Behavior of Hydroxyethyi Chitin Water Solution[J];Materials Review;2007-S3
3 Gao Shengji, Shen Baoluo, Chen Jian, Xiao Jianmei, Zhao Huancheng, Tu Mingjing (Dept. of Metallic Materials, Sichuan Union University, Chengdu 610065);Room Temperature-Tensile Strength of the Aluminium Matrix Composites Reinforced by Alumina-Silicate Fiber and Factors That Influence[J];RARE METAL MATERIALS AND ENGINEERING;1998-01
4 Li Gong;Zhou Zhenjun;Gao Yunpeng Wei Tong(The College of Materials Engineering,Yanshan University,Qinhuangdao 066004)(Yanshan Glass-making Factory, Qinhuangdao 066000)(Beidaihe Radio Factory, Qinhuangdao 066100);Preparation of Single-phase Mullite Fibers by Alkoxide Partly Hydrolysis[J];JOURNAL OF YANSHAN UNIVERSITY;1998-04
5 LIU Cong Hua 1,2 , DENG You Quan 1* , HUANG Quan 3, LI Qiang 3, GAO Xiong Hou 2, TAN Zheng Guo 2 (1. Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China; 2. Petrochemical Research Institute, Lanzhou Petrochemical Company of PetroChina, Lanzhou 730060, China; 3. Catalyst Plant, Lanzhou Petrochemical Company of PetroChina, Lanzhou 730060, China);Mullite Synthesis at Low Temperature and Its Crystal Structure Characterization[J];Chemical Research In Chinese Universities;2003-04
6 HAO Xiang-dong1; WANG Xin-wei2; ZHU Hong-bo2 (1. Refractory Materials Ltd., Changzhi Steel Group, Shanxi 046031, China; 2. College of Material Science & Engineering, Donghua University, Shanghai 200051, China);Preparation of aluminosilicate refractory fibers by using sol-gel process[J];Hi-tech Fiber & Application;2003-03
7 Tao Hungliang Yu Guiyu Yang Nauru (Nanjing Institute of Chemical Technology);Preparation of Unsupported γ-Al_2O_3 Separation Membrane by Sol-Gel Technique[J];Bulletin of the Chinese Ceramic Society;1994-01
8 Kong YongfaabYang ZhengfangbZhang WanlinaGong JianghongbZhang Guangyina a(Department of Physics,Nankai University)b(Advanced Ceramics Research Institute of Tianjin University);The Properties of Friction and Wear of Mullite Ceramics[J];BULLETIN OF THECHINESE CERAMIC SOCIETY;1999-04
9 ZHOU Feng-shan1, WANG Shi-hu2, SU Jin-zhu3, SUN Hu3, DING Jie1, XU Yi-zhuang1, WU Jin-guang1 1. College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, China 2. Research Institute of Production Technology, Shengli Oilfield, Dongying 257000, China 3. Downhole Technology Operation Company, Changqing Oilfield, Qingyang 745113, China;Structural Characteristics of Infrared Spectra for Polyaluminum Chloride in Enhanced Reactions of Modification[J];Spectroscopy and Spectral Analysis;2004-05
10 Su Chunhui Wang Yan Duanmu Qingduo (Material Department, Changchun College of Optics and Fine Mechanics, Changchun 130022) Zheng DafangSui Zhitong (Analysis Test Centre, Jilin University,(Colored Metallurgy Department, Northeast University, Ch;Study of Transparent Mullite Ceramic Film by XPS[J];ACTA OPTICA SINICA;1997-03
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