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《Journal of Synthetic Crystals》 2015-01
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Synthesis and Characterization of Bimetal Phosphide NiCoP by Reduction of Hypophosphite

TONG Jian-bo;LIU Ying-ying;LIU Shu-ling;College of Chemistry and Chemical Engineering,Shaanxi University of Science and Technology;  
Bimetal phosphide NiCoP was obtained from the reduction of hypophosphite salts using nickel nitrate hexahydrate(NiCl2· 6H2O), cobalt nitrate hexahydrate(CoCl2· 6H2O) and sodium hypophosphite(Na H2PO2·H2O) as material. The phase and structure of as-obtained samples were characterized by X-ray diffraction(XRD),field-emission scanning electron microscopy(FE-SEM),transmission electron microscopy(TEM) and N2adsorption-desorption analyses. The results show that the as-prepared NiCoP are hexagonal phase crystallographic particles with amorphous morphology,and the size of the particles ranges from 10-50 nm. The as-prepared bimetal phosphide NiCoP shows high activity in the adsorption removel property tests for some organic dyes.
【Fund】: 国家自然科学基金(21301113);; 陕西科技大学研究生创新基金资助项目
【CateGory Index】: TQ424
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