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《Plastics Additives》 2013-01
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Study on Synthesis of Calcium Acetylacetonate

Li Dui Zhang Hongliang Wang Yan Chen Xinhua Zhang Guoliang (Anhui Jiaxian Functional Additives Co.,Ltd.Bengbu,233010)  
The calcium acetylacetonate was synthesized using acetylacetone and new synthesised calcium hydroxide as raw materials,xylene as a dispersing agent.This method provides a new method for the synthesis of calcium acetylacetonate,and the optimum reaction conditions are,Ca (OH) 2,new synthesized,acetylaetone/Ca(OH) 2 mole ratio 1.5,dispersing agent:xylene,xylene/Ca(OH) 2 100 mL/0.1 mole,reaction temperature 110 ℃,reaction time 1 h.IR spectrum shows that acetylacetonate in the form of a monovalent anion with calcium ions forms ligand.XRD pattern shows that the substance is calcium acetylacetonate.
【CateGory Index】: TQ314.24
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