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《绍兴文理学院学报》 2005-01
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Supersonic Extraction of Laminaria and Scavenging Action to Free Radical

Liu Liping Zhong Yinfei (Department of Chemistry, Shaoxing University,Shaoxing,Zhejiang,312000)  
To study the optimization condition of extracting Laminaria with supersonic wave and scavenging action to free radical. We optimized the extraction factors with L9(34) orthogonal experimental design and measured its scavenging rate to hydroxyl free radical in Fenton system . The results showed that the optimal extracting technology was the mass ration of material to waters 1:40, supersonic power 200w, temperature 80 ℃, extracting time 45min and 3 times meanwhile. To compare it with the acid extracting method, the method can improve the extraction percentage of crude polysaccharide from 7.78% up to 10.26% and polysaccharide content from 16.74% up to 25.03% . The scavenging rate of the polysaccharide to hydroxyl free radical was to 72.6% while its concentration was 123.60μg/ml. The results indicate the polysaccharide has the stronger scavenging ability to hydroxyl free radical.
【CateGory Index】: TS254.4
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