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《Journal of Shenyang Pharmaceutical University》 1984-02
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THE DETERMINATION OF CURCUMOL IN THE VOLATILE OIL OF CURCUMA AROMATICA BY DUAL-WAVELENGTH TLC SCANNER

Li Jingkun Factory of Shenyang College of Pharmacy  
The separation of curcumol and other substances in the valatile oil of Curcuma aromatica was accomplished on silica gel CMC plate with petroleum ether (30—60℃) and ethyl acetate (95:5)as the developer. It is treated with 10% anillin-glacial acetic acid and perchloric acid(5:1), and then determined densitometrically with a Shimadzu CS-910 dual-wavelength TLC scanner. Reflection and linear scanning were adopted with λ_s being 515nm and λ_R, being 750nm. All data were recorded and calculated by a DM-6 recorder. This method which is simple and rapid gives stable and reproducible results.
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