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《Journal of Instrumental Analysis》 2008-07
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Synthesis and Characterization of Emodin Molecularly Imprinted Monolithic Column

YIN Yan-feng1,2,3,LI Juan-sheng1,YAO Yun-xian1,SHEN Hua1,CHEN Xiao-ming3(1.Changsha Environment Protection Technology College,Changsha 410004,China;2.Hunan Nantian Industry and Commerce Co.Ltd.,Xiangtan 411103,China;3.Institute of Chemistry and Chemical Engineering,Xiangtan University,Xiangtan 411105,China)  
A series of molecularly imprinted monolithic columns(MIMC) were synthesized using α-methacrylic acid as functional monomers,ethylene glycol dimethacrylate as crosslinker,the mixture of toluene and dodecadol as porogenic reagent and emodin as template molecules by in-situ polymerization.The trends of retention factors of imprinted and reference polymers were investigated.The MIMC synthesized under optimum conditions could efficiently separate emodin and its analogues.From the pore analytical data of molecularly imprinted polymer and reference polymer,it was found that there were two different kinds of pore distribution profiles in the former,whereas only one in the latter.
【CateGory Index】: R284
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