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《Journal of Instrumental Analysis》 2008-09
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Synthesis of Chloramphenicol Molecularly Imprinted Polymer and Its Analytical Application

WANG Rong-yan1,2,WANG Pei-long2,WANG Jing2,WANG Xi-chang1,ZHONG Yao-guang1 (1.College of Food Science and Technology,Shanghai Fisheries University,Shanghai 200090,China;2.Institute of Quality Standard and Testing Technology for Agro-Products,Chinese Academy of Agricultural Science,Beijing 100081,China)  
The method for synthesizing chloramphenicol molecularly imprinted polymer(CAP-MIP) and its optimal preparation conditions were studied.The surface structure of CAP-MIP was characterized by scanning electron microscope(SEM).The effects of the template to functional monomer ratio on the adsorptivity capacity of CAP-MIP were examined.The CAP-MIP was used as the filler for the solid phase extraction column.The selective adsorption of the column was then evaluated by the milk containing trace amount of CAP.Experimental results showed that the adsorptivity rate of CAP-MIP was up to 94.7% and the maximum adsorption capacity was 4 670 μg/g.
【Key Words】： chloramphenicol molecularly imprinted polymer adsorptive selectivity solid-phase extraction milk
【Fund】： “863”高新技术资助项目(2007AA10Z431)
【CateGory Index】： O631.3
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