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《Journal of Instrumental Analysis》 2008-10
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Molecularly Imprinted Polymer-Based Chemiluminescence for the Determination of Sudan Ⅰ

SHI Zuo-long,ZHANG Zhu-jun,SUN Yong-hua (School of Chemistry and Materials Science,Shaanxi Normal University,Xi′an 710062,China)  
Molecularly imprinted polymer(MIP) microspheres with a diameter range of 1-10 μm were synthesized by suspension polymerization using Sudan Ⅰ as the template molecule.An on-line preconcentration and extraction flow-injection system using solid phase extraction(SPE) column packed with prepared MIP microspheres was set up.The column was mounted on the 8-way valve of the flow injection system,and eluted with a mixture of methanol and formic acid(2∶1,by volume) after preconcentration.Sudan Ⅰ in the eluent was oxidized by acidic potassium permanganate in the flow cell forming a chemiluminescent product.Under optimal conditions,the chemiluminescence intensity has a linear relationship with the concentration of Sudan Ⅰ in the range of 1.0×10-6-7.0×10-4 g/L with a detection limit(3σ) of 3×10-7 g/L.The relative standard deviation was 2.0% for 1×10-5 g/L of Sudan Ⅰ(n=11).
【Fund】: 国家自然科学基金资助项目(30470886)
【CateGory Index】: TS207.3
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