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《Journal of Wuyi University(Natural Science Edition)》 2001-01
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Synthesis of adipates by Catalysis of Solid Acid under Microwave Irradiation

LI Nan1,FAN Xing-jun2,YUAN Ke-guo2,TAN Gan-zu2 (1. Dept. of Chem. and Env. Eng., of Wuyi Univ., Jiangmen 529020, China; 2. La nzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 ,China)  
:The synthesis of adipates were performed by esterification of adipic a cid and alcohol in catalysis of p-toluenesulfonic acid loaded on active carbon o r charcoal under microwave irradiation. The optimal reaction conditions were as follows:the mole ratio of adipic acid to alcohol was 1:4; the concentration of p-toluenesulphonic acid solution was 25%; the weights of catalyst, microwave po wer, and microwave irradiation time were 0.8g, 600W, and 45s respectively. The c onversion ratio of adipic acid in these reactions was high moreover the catalyst can be easily separated and used repeatedly.
【CateGory Index】: TQ414
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【Citations】
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9 ZHU Hong, HAN Wenfeng, CHAI Haifang, LIU Huazhang*(State Key Laboratory of Green Chemistry Synthesis Technology, Institute of Industrial Catalysis, Zhejiang University of Technology, Hangzhou 310014, Zhejiang, China);Preparation of Graphitic Carbon as Support of Ru-Based Catalyst for Ammonia Synthesis[J];Chinese Journal of Catalysis;2007-03
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1 ZHANG Yan-zong ZHENG Jing-tang QU Xian-feng CHEN Hong-gang (State key Laboratory of Heavy Oil,China University of Petroleum,Dongying 257061,China);The role of activated carbon in gas-liquid series electrical discharge reactor[A];[C];2007
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1 Wang Qiu-ying;ESTERIFICATION OF ACRYLIC DIOL CATALYZED WITH SOLID ACIDS[J];Paint & Coatings Industry;1983-02
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