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《Journal of Xi'an Jiaotong University》 2005-01
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Chemical Solid-Soluted Content of Strontium in Solid Solution of Hollandite

Teng Yuancheng~1,Zhou Shiguang~2,Xiao Zhengxue~2,Dong Faqin~1,Wang Chengduan~2 (1.Institute of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China; 2. Institute of Environment Engineering, Southwest University of Science and Technology, Mianyang 621010, China)  
Using SrCO_3,BaCO_3,Al_2O_3and TiO_2 as row materials,the single phase solid solution of hollan-dite of solid-soluted strontium was synthesized by the designed formulas and high temperature solid phase reaction. The design of formulas and the chemical solid-soluted content of strontium in solid solution of hollandite were investigated by X-ray diffraction, scanning electron microscope and wave dispersion spectrum. The experimental results indicate that the solid solution or single phase solid solution of hollandite with solid-soluted strontium can be easily synthesized by high temperature solid phase reaction, but the maximum chemical solid-soluted content of strontium is related to the design of formulas. It is 0.13 mol for the formula of Sr_xBa_1Al_(2+2x)Ti_(6-2x)O_(16),and 0.22 mol for the formula of Sr_(x+y)Ba_(1-y)Al_(2+2x)Ti_(6-2x)O_(16). The highest chemical solid-soluted amount of strontium in solid solution of hollandite is linked with synthesis method. The concentration of solid-soluted strontium in single phase solid solution of hollandite synthesized by homogeneous chemical reaction is higher than that by high temperature solid phase reaction. .
【Fund】: 国家自然科学基金委员会与中国工程物理研究院联合基金资助项目 (1 0 1 760 2 5)
【CateGory Index】: TL941
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