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《Journal of Southwest University(Natural Science Edition)》 2009-01
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Determination of Tetrahydropalmatine and Ferulic Acid in Tianqi Tongjing Capsules by HPLC

XIN Dan-min,ZHOU Guang-ming,HUANG Cheng,DENG Chuan-yue,LIANG Li-fang School of Chemistry and Chemical Engineering,Southwest University,Chongqing 400715,China  
An HPLC method is developed for the simultaneous separation and determination of tetrapalmatine and ferulic acid in the Chinese traditional patent medicine "Tianqi Tongjing capsules". Experiments were performed on a Hypersil C18 column (4.6 mm×150 mm,5.0 μm)and detected at 288 nm and at room temperature. The mobile phase was composed of methanol-0.002 mol/L postassium dihydrogen phosphate (40∶60) (pH was adjusted to 4.5 by phosphoric acid) at a flow rate of 0.8 mL/min. The linear range of tetrahydropalmatine and ferulic acid was 0.13-1.29 μg and 0.08-0.80 μg,respectively. The average recoveries of tetrahydropalmatine and ferulic acid were 97.96% (RSD=1.3%) and 98.47% (RSD=1.1%),respectively. It is concluded that the method can be successfully applied in quality control of Tianqi Tongjing capsule,which has proved to be accurate,simple,effective and reproducible.
【Fund】: 重庆市自然科学基金资助项目(CSTC2007BB5370)
【CateGory Index】: R286
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