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《Journal of Southwest University(Natural Science Edition)》 2009-01
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Determination of Sodium Cyclamate in Foods with Capillary Column Gas Chromatography

MEI Wen-quan1,2,LI Qi-wan1,2,WANG Lu-xiang1,2,YANGJu1,21. Quality Standardizing and Testing Technology Institute,Yunnan Academy of Agricultural Science,Kunming 650223,China;2. Supervision & Testing Center for Farm Products Quality,Ministry of Agriculture,Kunming 650223,China  
A method for determinating sodium cyclamate in foods was developed. The sodium cyclamate in the food samples was extracted with a homogenizer. Under the optimized chromatograph conditions,the sodium cyclamate in the foods was separated by weak-polar capillary column (HP-5),and determined by a fire iron detector (FID). The result showed that the standard curve met the linear equation Y=0.000 4X+6.185 2,and the correlation coefficient was 0.999 6. The average recovery ranged from 94.9% to 98.5%,and the relative standard deviations (RSDs) were 0.71%-3.70%. The minimum detection limit was 2 mg/L and 20 mg/kg in the drink samples and solid samples,respectively.
【CateGory Index】: TS207.3
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