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《Journal of Southwest China Normal University(Natural Science Edition)》 2006-06
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The Effective Method of Synthesis of 2-Aryloxy-5-Chloro-Aminobenzene

LIU Jing-zi~1,SHI Da-bin~1,WANG Yu-liang~2,CHEN Shu-hua~21.Dept.of Pharmic Chemistry,Zun yi Medical College,Zunyi Guizhou 563003,China;2.The Faculty of Chemistry,Sichuan University,Chengdu 610064,China  
A series of 2-aryloxy-5-chloro-aminobenzene were synthesized by the reaction of 2-aryloxy-5-chloro-nitrobenzene with the reducing agent sodium sulfide.The method has the advantages of high yield,simplicity in operation and few by-product.In addition,sodium sulfide is cheap,facile and environment-friendly.It shows that the choice of reducing agent on organic synthesis has economical and theoretical value.All the compounds were characterized by elemental analysis,IR,(~1H) NMR and MS.
【CateGory Index】: TQ246
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