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《Chinese Journal of Applied Chemistry》 2005-11
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Synthesis and Properties of Quinine Imprinted Polymer Bound on Silica

HE Jian-Feng~(a,b),LIU Lan~a,LUO Yong~a,YANG Gui-Lan~a,DENG Qin-Ying~(a*)(~aSchool of Chemistry and Chemical Engineering,Sun Yat-san University,Guangzhou 510275;~bCollege of Pharmacy,Guangzhou University of TCM,Guangzhou)  
With micro-porous silica functioned with 3-(trimethoxysilyl)propyl methacrylate reagent as carrier,a kind of novel molecularly imprinted polymer bound on silica surface was synthesized by using MAA and(quinine) as functional monomer and template respectively.The polymer was characterized by IR and SEM.MAA and (quinine) could interact to form super-molecular complexes,which were confirmed by fluorescence and UV spectroscopy.The adsorption properties of the polymers toward substrates were evaluated by(equilibrium) adsorptive experiments.The results show that there exist distinct difference between the template polymer and the control polymer,the maximum special adsorption amount toward template is 36.40 μmol/g.The separation factor reaches 1.64 for quinine and cinchonine.
【Fund】: 国家自然科学基金(20202015);; 国家教育部博士点基金(20020558026)资助项目
【CateGory Index】: O631.3
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