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《Chinese Journal of Applied Chemistry》 2007-03
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Molecularly Imprinted On-line Solid-phase Extraction Combined with Flow Injection Chemiluminescence for Determination of Chlortetracycline

YANG Chun-Yan, XIONG Yan, HE Chao, ZHANG Zhu-Jun (School of Chemistry and Chemistry Engineening,Southwest Normal University,Chongqing 400715)  
Chlortetracycline hydrochloride can enhane the chemiluminescence of Ce(Ⅳ) and Rh6G in acidic medium. So novel molecularly imprinted polymer solid-phase extraction(MISPE) method combined with flow-injection chemiluminescence for determining chlortetracycline hydrochloride was developed. The MIP was synthesized by using tetracycline as the imprinting molecule which has a structure similar to that of chlortetracycline. A polytetrafluoroe-thylene(PTFE) tube packed with the particles of MIP was employed as an MISPE micro-column and was connected to the sampling loop of the eight-way injection valve for the preconcentration and extraction of chlortetracycline hydrochloride. The eluent was used as the carrier for extracting the adsorbed chlortetracycline hydrochloride to react with a mixture of cerium(Ⅳ) and rhodamine6G in the flow cell to produce strong CL. Intensity of CL is linearly changed with the concentration of chlortetracycline hydrochloride from 2×10-8 g/mL to 1×10-6 g/mL and the limit detection is 4×10-9 g/mL(3σ). This method has been successfully applied to the determination of chlortetracycline hydrochloride in liver of chicken sample.
【Key Words】： molecularly imprinted polymer solid phase extraction chemiluminescence flow-injection chlorte-tracycline
【Fund】： 国家自然科学基金资助项目(30470886)
【CateGory Index】： TQ465
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