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《Yunnan Journal of Traditional Chinese Medicine and Materia Medica》 2014-07
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Study on the Compositions of Flavonoid Glycosides of Epimedium Koreanum Leaves

LI Jin-yu;LI Hong-mei;LI Rong-tao;School of Life Science and Technology,Kunming University of Science and Technology;  
Objective: To study the chemical composition of Epimedium koreanum leaves. Methods: The silica gel column chromatography,Toyopearl,Sephadex LH- 20 column chromatography,ODS column chromatography and reversed- phase HPLC chromatography were used to separate and purify Epimedium koreanum and its structures were identified and analyzed through the physical and chemical properties and spectral data. Results: Six flavonoid glycosides were isolated from the dried leaves of 70% of acetone /water extracts,and identified as(1)chrysoeriol- 7- O- β- D- glucuronic acid- 6"- methyl ester,(2)apigenin- 7- O- β- D- glucuronide- 6"- methyl ester,(3)3',5,7- trihydroxy- 4'- methoxy flavone- 3- O- α- L- rhamnopyranosyl(1 →6)- β- D- glucopyranoside,(4)kaempferol- 3- O- α- L- pranrhamnose base(1→6)- β- D- glucopyranoside,(5)rutin and(6) quercetin- 3- O- β- D- galactose- 7- O- β- D- glucopyranoside. Conclusion: The compound 1 and 2 were isolated from Epimedium genus plant for the first time and the compound 3,4 and 6 were isolated from this plant for the first time.
【Fund】: 国家自然科学基金(NO:21262021)
【CateGory Index】: R284.1
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