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《Chinese Tobacco Science》 2015-01
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Determination of Twelve Common Pesticides Residues in Tobacco by Using Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

XIONG Wei;SHAO Jimin;PANG Su;HUANG Mei;TAO Xiaoqiu;Sichuan Tobacco Quality Supervision and Testing Station;  
In order to rapidly determine common pesticide residues in tobacco, a rapid method for determining twelve pesticides in tobacco using UPLC-MS/MS was developed. Samples were extracted by acetonitrile, cleaned up by dispersive solid-phase extraction and finally detected by UPLC-MS/MS. The results showed that the recoveries of twelve pesticides ranged from 62.1%-126.3% at the spiking levels of 20 μg/kg, 200 μg/kg and 500 μg/kg. The RSD ranged from 0.6%-14.8%, and the LOD was from 0.24 μg/kg to 4.24 μg/kg. For the superior sensitivity, targeted residues and shorter analysis time, this method was suitable for the rapid analysis of common pesticide residues in batches of tobacco samples.
【Fund】: 四川省烟草专卖局(公司)科技计划项目(201301003)
【CateGory Index】: S481.8
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