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《Chinese Journal of Pharmaceuticals》 2011-06
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Determination of Four Components in Zushima Guanjie Zhitong Strappings by Capillary Gas Chromatography

ZHANG Yiming,GUO Pu,WANG Jie,HU Mingxun,CHEN Anjia(College of Pharmaceutical Sciences,Shanxi Medical University,Taiyuan 030001)  
A capillary gas chromatography was established for the determination of camphor,menthol,borneol and methyl salicylate in Zushima Guanjie Zhitong strappings.n-Octanol was used as the internal standard.The sample solution was prepared by distillation with essential oil collector.A PEG-20M capillary column was used with a flame ionization detector.The calibration curves of camphor,menthol,borneol and methyl salicylate were linear in the concentration ranges of 30-480,35-560,33-520 and 30-472 μg/ml.The average recoveries were 99.2%,99.1%, 99.1% and 99.0%,with RSDs of 0.8%,0.7%,0.9% and 1.1%,respectively.
【Key Words】: camphor menthol borneol methyl salicylate Zushima Guanjie Zhitong strappings capillary gas chromatography determination
【Fund】: 山西省自然科学基金项目(2008011077-1)
【CateGory Index】: TQ461
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【Citations】
Chinese Journal Full-text Database 4 Hits
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【Co-citations】
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1 DENG Zu-lei,ZHANG Qing-yun(Bengbu Institute for Food and Drug Control,Bengbu Anhui 233000);Determination of menthol in Qinghuo tablet by GC[J];Anhui Medical and Pharmaceutical Journal;2008-08
2 NI JI-hong,PAN Ze-hua,XIE Hong-xing(Anhui Anke Yuliangqing Pharmaceutical Co.,Ltd.,Anqing 246005,China);Determination of camphor in shexiang zhentong plaster by GC[J];Anhui Medical and Pharmaceutical Journal;2009-02
3 DU Wei-feng1,LI Lei1,MA Hong-yi2(1.Anhui Institute for Food and Drug Control,Hefei 230051;2.Bengbu Institute for Food and Drug Control,Bengbu 233000);Determination of beclomethasone dipropionate in cremor mentholi compositus by HPLC with internal standard[J];Anhui Medical and Pharmaceutical Journal;2009-02
4 YI Wen-min1,WANG Xiu-yue2 (1.Fuyang Cancer Hospital,2.Fuyang Institute for Drug Control,Fuyang 236000);Determination of borneol in xiaomi suppository by gas chromatography[J];Anhui Medical and Pharmaceutical Journal;2010-04
5 DENG Zu-lei,ZHANG Qing-yun(Anhui Bengbu Institute for Food and Drug Control,Anhui,Bengbu,233000,China);Determination of menthol in compound Sangju cold granules by GC[J];Strait Pharmaceutical Journal;2010-10
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7 Ouyang Wei,Liu Xuping,Chen Jianlan1 and Zeng Chen1(Jiangxi Institute for Control of Food and Drug,Nanchang 330046;1Jiangxi University of Chinese Traditional Medicine);Determination of Impurity Camphor in Natural Borneol(d-Borneolum) by GC[J];Chinese Pharmaceutical Affairs;2010-02
8 ZHANG Yi-ming,WANG Jie,HU Ming-xun,HAO Zeng-yan,CHEN An-jia(College of Pharmaceutical Sciences,Shanxi Medical University,Taiyuan 030001,China);Determination of Four Active Components in Hongyao Strapping by Capillary Gas Chromatography[J];Chinese Journal of Experimental Traditional Medical Formulae;2011-07
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