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《Occupation and Health》 2012-04
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Research on detection method of pesticides residues of organic phosphorus and carbamate in vegetables and fruits

HAO Ning Physical and Chemical Laboratory,Handan Center for Disease Control and Prevention,Hebei,056008,China  
[Objective]To establish a method for rapidly detecting 16 kinds of pesticides residues of organic phosphorus and carbamate in vegetables and fruits[Methods]The detection was conducted by applying gas chromatography with quartz capillary,by using nitrogen-phosphorus detector with high sensitivity and through extracting sample by acetonitrile and acetone.[Results]the linear ranges of organophosphorus pesticides were 5.0-1 000.0 μg/kg,r≥0.999 0.The lowest determination limit was 0.1-0.5 μg/kg,the recoveries were 66.0%-84.0%,and RSD was 4.8%-9.5% [Conclusion]This method can determine organic phosphorus and carbamate pesticides simultaneously in vegetables and fruits.It has the characteristics of high sensitivity,good separating effect,high recovery rate,small variance coefficient and low determination limit.
【CateGory Index】: R155.5
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Chinese Journal Full-text Database 4 Hits
1 LIU Manman1,2,KANG Shu2,YAO Cheng1(1.College of Science,Nanjing University of Technology,Nanjing 210000,China; 2.Beijing Purkinje General Instrument Co.,Ltd,Beijing 101200,China);Research progress of QuEChERS method in pesticide mult-residue analysis[J];Chinese Journal of Pesticide Science;2013-01
2 XU Yuan-ming,ZHANG Zhen-fa(Department of Chemical and Biological Engineering,Guangxi Normal University for Nationalities,Chongzuo 532200,Guangxi,China);Determination of Organophosphorus Residues in Cassava by GC/FID[J];Hubei Agricultural Sciences;2013-09
3 Cai Wei,Zhang Yan,Liang Dong (College of the Mechanical and Electrical Engineering,Hainan University,Haikou 570228,China);Mechanical Design and Test Based Water Jet Potato Cleaning[J];Journal of Agricultural Mechanization Research;2013-09
4 WANG Jun,ZENG GUAN You-zhi, YU Wei,et al. Physiochemical Laboratory of Shenzhen Municipal Chronic Disease Center,Shenzhen 518020,Guangdong, P. R China;Detection of pesticides residues of carbamate in vegetables by GC-MS[J];China Tropical Medicine;2013-02
Chinese Journal Full-text Database 2 Hits
1 PAN Shou-qi,SUN Jun,DONG Jing,LIU Yong-qiang and REN Fang(Weifang Entry and Exit Inspetion and Quaratine Bureau,Weifang 261041);Determination of 24 organophosphorus pesticide residues in vegetable by gas-chromatography[J];Chinese Journal of Analysis Laboratory;2010-01
2 LI Yao-xin, DONG Quan (College of Food Science, Southwest University, Chongqing 400715);Detection Technical Progress of Organophosphorus Pesticide Residue[J];Food and Nutrition in China;2010-04
Chinese Journal Full-text Database 10 Hits
1 LIU Hui,CAO Zhao-yun,ZHANG Li-qiang and CHEN Ming-xue(Rice Product Quality Supervision and Inspection Center,China National Rice Research Institute,Ministry of Agriculture,Hangzhou 310006);Determination of haloxyfop-etotyl in agricultural products by dispersive solid phase extraction and liquid chromatography-mass spectrometry[J];Chinese Journal of Analysis Laboratory;2011-03
2 Fu Ruo-nong(Depertment of Chemistry,Beijing Institute of Technology);The advances of gas chromatography in recent two years[J];Chinese Journal of Analysis Laboratory;2011-05
3 XU Guo-feng,NIE Ji-yun*,LI Hai-fei,LI Jing,WU Yong-long(Research Institute of Pomology,Chinese Academy of Agricultural Sciences,Xingcheng,Liaoning 125100 China);Effects of matrix on analysis of organophosphorus pesticide residue in pear and apple by gas chromatographic methods[J];Journal of Fruit Science;2011-01
4 XING Hong-xing1,PAN Xiao-wei2,HUANG Yong-ping3,WANG Li-rong2(1.Analysis and Testing Center,CATAS of Hainan Province,Haikou 571101,China; 2.College of Food Science of Technology Hainan University of Hainan Province,Haikou 570228,China; 3.The Station of Plant Proctection and Quarantine of Hainan Province,Haikou 570203,China);Applicatior of Residue Detection Technology in Organophosphorus Pesticide[J];Analysis and Testing Technology and Instruments;2012-04
5 LIN Qi-da(Shenzhen Quality Supervision and Inspection Station of Green Agricultural Products,Guangdong 518040,PRC);Degradation Dynamics and Residue Analysis of Buprofezin in Rice Plant[J];Hunan Agricultural Sciences;2011-03
6 SHEN Dan-yu1,TANG Fu-bin1,ZHONG Dong-lian1,SHEN Li2,MO Run-hong1(1.Research Institute of Subtropical Forestry,Chinese Academy of Forestry,Zhejiang 311400,PRC; 2.Fuyang Test Center of Quality and Metrology,Zhejiang 311400,PRC);Determination of 14 Organophosphorus Pesticides' Residues in Coprinus comatus by QuEChERS-Gas Chromatography[J];Hunan Agricultural Sciences;2011-21
7 ZHANG Jie,XU Jia-sheng,LIU Lian-li(Center of Science and Technology Experiment,Bohai Univer,Jinzhou 121013,P.R.China);Rapid Determination of Phorate and Mmethyl Parathion Residues in Vegetables and Fruits by Gas Chromatography[J];Science Technology and Engineering;2011-13
8 ZHU Xue-liang2,QI Xiang-yang1,2,LIU Chuan-ju2,LI Hui-hui2,LIU He-sheng2,CAO Pin-bao2,WANG Jing2(1.Dept.of Biological Environmental Sciences,Zhejiang Wanli College,Ningbo 315100,China;2.College of Food Science and Technology,Huazhong Agricultural University,Wuhan 430070,China);GC Determination of 3 Residual Fungicides in Peach with Matrix Solid Phase Dispersion of Sample[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2009-01
9 HUANG Bao-yong~(1,2), OUYANG Xi-hui~2,PAN Can-ping~(1*)(1.College of Science,China Agricultural University,Beijing 100094,China;2.Beijing Municipal Station of Agro-Environmental Monitoring,Beijing 100029,China);Matrix Effects in the Analysis of Pesticide Residue in Agro-products by Chromatographic Methods[J];Chinese Journal of Pesticide Science;2005-04
10 Cai Wei,Zhang Yan,Liang Dong (College of the Mechanical and Electrical Engineering,Hainan University,Haikou 570228,China);Mechanical Design and Test Based Water Jet Potato Cleaning[J];Journal of Agricultural Mechanization Research;2013-09
China Proceedings of conference Full-text Database 1 Hits
1 Zhu Xujun, Hou Ruyan* (Key Laboratory of Tea Biochemistry & Biotechnology, Ministry of Education and Ministry of Agriculture, Anhui Agricultural University, Hefei 230036,China);Advances in the Determination of Pesticide Residues in Tea[A];[C];2007
Chinese Journal Full-text Database 10 Hits
1 PENG Jin-yun et al(Department of Chemistry and Biological Science,Guangxi Normal University of Nationalities,Chongzuo,Guangxi 532200);Determination of Residues of Organophosphorus in Sugarcane by FID/GC[J];Journal of Anhui Agricultural Sciences;2010-03
2 YANG Jing~(1,2),CAO Hai-feng~1 (1.Northeast Agricultural University,Harbin,Heilongjiang 150030(2.Safety of Agriculture Products Quality Testing Center of Harbin, Harbin,Heilongjiang 150070);Determination of 14 Organ Phosphorus in Cucumber of Green Vegetables by Using Gas Chromatography[J];Northern Horticulture;2012-12
3 Zhang li,Wu ye,Xiao bing,Li xiao-dong,Chen hong(Faculty of Materials Science and Chemical Engineering,China University of Geosciences,Wuhan,Hubei 430074,China);Research New Progress of Supercritical Fluid Extraction Technology[J];Fujian Analysis & Testing;2009-02
4 JIANG Jun1,3,LI Pei-Wu* 1,2,3,XIE Li-Hua1,DING Xiao-Xia1,2,LI Ying1,3,WANG Xiu-Pin1,3,WANG Xue-Fang1,3,ZHANG Qi1,3,GUAN Di1,3 1(Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062) 2(Key Laboratory of Oil Crop Biology of the Ministry of Agriculture,Wuhan 430062) 3(Quality Inspection and Test Center for Oilseeds Products,Ministry of Agriculture,Wuhan 430062);Rapid Screening and Simultaneous Confirmation of 64 Pesticide Residues in Vegetable Using Solid Phase Extraction-comprehensive Two-dimensional Gas Chromatography Coupled with Time-of-Flight Mass Spectrometer[J];Chinese Journal of Analytical Chemistry;2011-01
5 LU Dan-Feng1,LIU Rui-Peng1,QI Zhi-Mei1,2(1State Key Laboratory of Transducer Technology,Institute of Electronics,Chinese Academy of Sciences, 2State Key Laboratory On Integrated Optoelectronics,Beijing 100190);An Optical Method for Rapid Detection of Organophosphates Based on Multilayer-Disc Sensing Element[J];Chinese Journal of Analytical Chemistry;2011-06
6 DONG Jing1,PAN Yu-xiang1,QIN Ya-ping2,YU Qiong-wei3,LUO Dan3 (1.Weifang Entry-Exit Inspection and Quarantine Bureau,Weifang 261041;2.Beijing Micromole Separation Testing Technology Co.,Ltd.,Beijing 100191;3.College of Chemistry and Molecular Sciences,Wuhan University,Wuhan 430072);Simultaneous Determination of 103 Pesticide Residues Using Gas Chromatography-Negative Chemical Ionization Mass Spectrometry[J];Journal of Analytical Science;2010-03
7 WU Jian-wei1,2,XU Rong1,ZHAO Run-huai2,CHEN Bo2,CHEN Jun1(1.Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences, Peking Union Medical College,Beijing 100193; 2.Technology development center,China National Group Corp.of Traditional & Herbal Medicine,Beijing 102600);Analysis of Pesticide Residues Using the Quick Easy Cheap Effective Rugged and Safe(QuEChERS) Pesticide Multiresidue Method in Fifty Traditional Chinese Medicine by Gas Chromatography[J];Journal of Analytical Science;2011-02
8 WANG Jian hua * (Shandong Impostand Export Commodity Inspection Bureau,Qingdao 266002), WANG Guo tao and YUAN She mei (Shengli Oil Transportation Company,Weifang),Fenxi Shiyanshi,1999,18(6):55~58;Supercritical Fluid Extraction Gas Chromatographic Determination of Organophosphorus Pesticides in Vegetables and Fruits[J];ANALYTICAL LABORATORY;1999-06
9 ZHANG Mao-sheng1,2,GONG Li-fen1,3,YU Bin-bin1,ZENG Jing-bin1,YUAN Ning1 and CHEN Xi*1(1.Department of Chemistry and the Key Laboratory of Analytical Sciences of the Ministry of Education,College of Chemistry and Chemical Engineering,Xiamen University,Xiamen 361005;2.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Zhangzhou 363000;3.School of Chemistry and Life Science,Quanzhou Normal University, Quanzhou 326000);Determination of organochlorine and pyrethroid pesticides in vegetable samples by ultrasonic extraction and SPME-GC method[J];Chinese Journal of Analysis Laboratory;2008-04
10 WEI Shan-ming1,ZHOU Wei*2,JIN Ming3,LI Li-ping1 and XU Ying4(1.The Geography and Environment Science College of Northwest Normal University,Lanzhou 730070;2.Gansu Entry-Exit Inspection & Quarantine Bureau,Lanzhou 730020;3.Gansu Agriculture University Faculty of Food Science and Technology,Lanzhou 730070;4.Lanzhou Institute of Biological Products,Lanzhou 730046);Determination of OPPs residues in vegetables by non-equilibrium SPME coupled to GC[J];Chinese Journal of Analysis Laboratory;2008-06
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Rong et al(Anhui Key Laboratory of Agro-food Safety,Resource and Environmental College of Anhui Agricultural University,Hefei,Anhui 230036);Study on Separation of 6 Kinds of Organophosphorous Pesticides and Determination of Their Residues in Water by HPTLC[J];Journal of Anhui Agricultural Sciences;2009-14
2 QUE Mu-wang (Wellink Chemical Iudustrial Co.,Ltd.,Nanping 353000,china);Study on the Determination of Organophsphorus Pesticides Using Micellar Electrokinetic Capillary Chromatography(MEKC)[J];Chemical Engineering & Equipment;2008-10
3 ZHANG Zhuo-min1,2,CHEN Jin-quan1,2,ZHANG Lan1,31.Key Laboratory of Analysis & Detection for Food Safety(Fuzhou University) Ministry of Education,Fuzhou 350002,China;2.College of Chemistry and Chemical Engineering,Fuzhou University,Fuzhou 350002,China;3.The Sport's Science Research Center of Fuzhou University,Fuzhou,350002, China);Determination of Five Organophosphorus Pesticides in Vegetables by Solid Phase Extraction-High Performance Liquid Chromatography[J];Analysis and Testing Technology and Instruments;2008-02
4 Lu Yinghua, Chen Yanjun , Jia Shaohui,et al (Department of Chemistry, Jining Medical Collage);DETERMINATION OF RESIDUE AND DEGRADATION OF PROFENOFOS IN RAPES[J];Journal of Jining Medical College;2003-03
5 HUANG Su-fang1,ZHU Yu-jing1,LIN Kang-mei 1,LAN Jiang-lin1,LI Fang2,SHI Huai 1,LIU bo1(1.Biotechnology Institute,Fujian Academy of Agricultural Sciences,Fuzhou 350003,China;2.Departmental of Plant Protection,Fujian Agricultural and Forest University,Fuzhou 350002,China);Study on the Residue of Chlorpyrifos in Ipomoea aquatica Forsk and the Soil[J];Journal of Agro-Environment Science;2006-S1
6 Liu Chunlai(College of Bio- Safety Science and Technology, Hunan Agriculture University,Changsha 410128)Li Suping,Hu Changdi,Liu Zhaoqing,ZhangXianghui(Institute for the Control ofAgrochemicals,Hunan Province,Changsha 410005);Study on Residue Dynamic of Triazophos in Cabbage[J];Pesticide Science and Administration;2005-05
7 WU Min,HU Xiou-qing,ZHAO Hua,ZHU Ya-hong,XU HaoPING Li-feng,WANG Xin-quan,LI Zhen(Institute of Quality and Standard for Agricultural Products,Zhejiang Academy of AgriculturalSciences,Hangzhou 310021,China);Field Residue Decline Study of Acephate and Methamidophos in Crop and Soil[J];Chinese Journal of Pesticide Science;2009-01
8 WU Hua, LI Bing-qing, LIN Qiong-fang, HUANG Hong, OU Jian-feng, LIU Gui-qing (Guangdong Entomological Institute, Guangdong Public Laboratory of Protection and Utilization of Wild Animal, Guangzhou 510260, China);The Residue Dynamic of Chlorpyrifos in Carob, Chili and Soil[J];Agrochemicals;2007-11
9 PAN Jian,XIA Xiao-xiao,YANG Yi,LIANG Juan (Engineering Research Center of Bio-process, Ministry of Education, Hefei 230009, China);Rapid Analysis of 13 Organophosphorus Residues of Pesticides in Spinach by Liquid Chromatography-Electrospray Tandem Mass Spectrometry[J];Food Science;2008-04
10 CHEN You-gen1,YANG Mei-hua2,,GUO Hong-zhu1,WANG Zhi-bin1 (1.Beijing Institute for Drug Control,Beijing 100035 China;2.Institute of Medicinal Plant Development,College of Peking Union Medical,Chinese Academy of Medical Sciences,Beijing 100193 China);Simultaneous Determination of Contents of Five Kinds of Orgnaophosphorus Pesticides Residues in Grains and Vegetables with Capillary Gas Chromatography[J];Food Science;2008-12
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