Fabrication of Al_(2(1-x))Mg_xTi_(1+x)O_5 Composite Powder by Chemical Co-Precipitation
Yang Rui Shen Shangyue (Dept. of Materials Science and Chemical Engineering ,China University of Geo sciences, Wuhan 430074) Shen Qiang Wang Chuanbin Zhang Lianmeng (State Key Lab. of Advanced Technology for Materials Synthesis Processing, Wu han University of Technology , Wuhan 430070)
By using chemical co- precipitation method, Al2(1- x)MgxTi1+ xO 5 composite powder was fabricated from TiCl4, MgCl2 and AlCl3 solutions with NH3 (H2O, NH4HCO3 as the precipitators. The properties of the powder were characteri zed by TG- DTA, XRD and calculation of the crystal lattice constant. All the re sults indicate that the thermal stability of Al2TiO5 obtained by chemical co- p recipitation is effectively enhanced compared with that fabricated by solid- st ate synthesis method. The optimum conditions for preparing Al2(1- x)MgxTi1+ xO5 composite powder are 30mol% MgTi2O5, 2mol/L NH3· H2O, pH of 9 and calcin ation temperature of 1350℃ .